A kind of oxide containing lithium tungsten bronze structure as visible effect photocatalyst, the chemical formula of lithium tungsten bronze structure oxide is = Ba5LiFe0.5 (NbxTah) λ A. (0 <x <1) preparation steps of lithium tungsten bronze structure oxide are as follows: mix the 99.9% analytically pure chemicals of BaCO3, Li2CO3, Fe2O3, Nb205 and Ta2O5 as formula Ba5LiFe0.5Nb4.75Ta4. 75 O30, put into the mill pot, add zirconia balls and ethanol, milling for 2-8 hours, mix grinding, remove and dry through 200-mesh sieve; the resulting powder material calcine at 1175-1275 ℃, and incubate for 6-8 hours, cool to room temperature, and then pulverized by ball mill so that the particle size gets smaller to 2 μm, then the lithium tungsten bronze structure oxide powder Ba5LiFe0.5Ta9.5O30 is obtained, 0 <x <10. This method is simple, with low cost, photocatalys obtained has excellent catalytic performance, with effects of decomposing harmful chemical substances, organic biomass and bactericidal under visible light irradiation.
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